PURPOSE FOR THE COURSE
Get acquainted with methods for characterization of coarse disperse system, to transformations that occur during mechanical activity and to study their effect on the response of each separation process and mixing technology.
To adopt the fundamentals that ensure proper estimation and selection of optimal thermal separation process with reference to energy savings and environmental impact.
CONTENTS FOR THE COURSE
The 1st week Opening lecture, Students will be introduced to teaching and knowledge testing for this course, Mechanical and thermal separation processes (the key characterics, their differences), Fundamentals of mechanical macroprocesses, Characterization of coarse disperse systems
The 2nd week Fundamentals of mechanical separation, Gravitational and centrifugal sedimentation, Equipment selection
The 3rd week Filtration, Macrofiltration types, Filtration equipment selection
The 4th week The 1st partial exam
The 5th week Mixing of liquids and suspensions, Design and scaling of process unit for mixing, Mixing of powders (units, equipment selection)
The 6th week Comminution
The 7th week The 2nd partial exam
The 8th week Basics of thermal separation processes. Heat exchangers.
Calculation examples.
The 9th week Evaporation. Methods of energy savings in evaporation. Equipment classification and selection. Calculation examples.
The 10th week Crystallization. Kinetics, nucleation and growth mechanisms. Equipment classification. Calculation examples.
Lab assignment III: Crystallization
The 11th week Drying. Kinetics and mathematical description of the process. Energy savings. Equipment classification. Calculation examples.
The 12th week The 3rd partial exam
The 13th week Distillation. Implementation methods. Column design (height, diameter, number of theoretical units). Calculation examples.
Lab assignment IV: Drying
The 14th week Absorption and Extraction. Methods of process implementation. Equipment classification. Calculation examples.
The 15th week The 4th partial exam
GENERAL AND SPECIFIC COMPETENCE
Acquiring knowledge necessary for analysis of complex processes to a more simple units (units of mechanical and thermal process engineering).
RESPONSIBILITIES FOR THE STUDENTS AND METHODS TO DO SO
Regularly attending classes (lectures, seminars and lab tutorials), writting the lab reports and homeworks.
CRITERION TO ACCESS THE TEST
Regularly attending lecturs and seminars (75 %), and successfully finished lab tutorials and homeworks delivered on time.
TEACHING MODI
lectures,
seminars - calculations
lab tutorials
consultations if there is a need
KNOWLEDGE TESTING AND EVALUATION
4 partial exams and entrance tests for the lab tutorials.
MONITORING OF THE COURSE QUALITY AND SUCCESSFULNESS
By student questionnaire.
METHODICAL PRECONDITIONS
Exams for the courses Transport phenomena and Mass and energy balance with positive scores.
LEARNING OUTCOMES FOR THE COURSE
1. To scan the dispersity state of coarse disperse systems.
2. To calculate the efficiency parameters in processes of mechanical separation.
3. To predict the progress of separation process, needed separator area, time and driving force for the process by using mathematical descriptions of underlying phenomena.
4. To design and scale of units for successfull mixing in real and set conditions.
5. To analyse comminution kinetics using population balance approach.
6. To distinguish different thermal separation processes
7. To identify the need for energy and or mass separating agent for a particular separation process.
8. To differentiate mechanisms for mass and heat transfer and the corresponding resistances in a particular separation process.
9. To evaluate the feasibility of separation process.
LEARNING OUTCOMES FOR THE STUDY PROGRAMME
1. To explain scientific principles important for materials science and engineering, especially in the field of chemistry, physics, mathematics and chemical engineering.
2. To solve calculation problems by correct use of physical units and thermodynamic tables.
3. To theoretically explain result of experimental work.
4. To optimise chemical and other industrial processes applying chemical engineering methodology.
LITERATURE
1 M. Rhodes, Introduction to Particle Technology, John Wiley & Sons, West Sussex, 2008. A. Rushton, A.S. Ward, R.G. Hodlich: Solid - Liquid Filtration and Separation Technology, VCH Weinheim 1996. K.Satler, H.J.Feindt, Thermal Separation Processes - Principles and Design, VCH Verlagsgesellschaft mbH, Weinheim; 1995. J.D.Seader, E.J. Henley, Separation Process Principles, John Wiley & Sons, Inc., 2006. - optional literature
2 Krunoslav Žižek and Aleksandra Sander. Course materials in PDF (available on the web sites of the Faculty of Chemical Engineering and technology and Merlin system for e-learning) - mandatory literature
3 Aleksandra Sander. Internal script: Toplinski separacijski procesi i Priručnik za vježbe iz Toplinskih separacijskih procesa (available on the web sites of the Faculty of Chemical Engineering and technology and Merlin system for e-learning) - mandatory literature
4 Gordana Matijašić. Priručnik za vježbe iz Mehaničkih separacijskih procesa (available on the web sites of the Faculty of Chemical Engineering and technology and Merlin system for e-learning) - mandatory literature
5 K. Satler, H.J. Feindt. Thermal Separation Processes - Principles and Design, VCH, Weinheim1995. - optional literature
6 M. Hraste. Mehaničko procesno inženjerstvo, Hinus, Zagreb 2003. - optional literature.
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Nastavni materijali u PDF obliku, Objavljeni na mrežnim stranicama Fakulteta i Merlin sustava za e-učenje.., Izv. prof. dr. sc. Krunoslav Žižek i prof. dr. sc. Aleksandra Sander,
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Interne skripte: Toplinski separacijski procesi i Priručnik za vježbe iz Toplinskih separacijskih procesa, Dostupno na mrežnim stranicama Fakulteta i Merlin sustava za e učenje., Prof. dr. sc. Aleksandra Sander,
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Priručnik za vježbe iz Mehaničkih separacijskih procesa, Dostupno na mrežnim stranicama Fakulteta i Merlin sustava za e učenje., Prof. dr. sc. Gordana Matijašić,
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M. Rhodes, Introduction to Particle Technology, John Wiley & Sons, West Sussex, 2008.
A. Rushton, A.S. Ward, R.G. Hodlich: Solid - Liquid Filtration and Separation Technology, VCH Weinheim 1996.
K.Satler, H.J.Feindt, Thermal Separation Processes - Principles and Design, VCH Verlagsgesellschaft mbH, Weinheim; 1995.
J.D.Seader, E.J. Henley, Separation Process Principles, John Wiley & Sons, Inc., 2006.,
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Thermal Separation Processes - Principles and Design, VCH, Weinheim1995., K. Satler, H.J. Feindt,
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Mehaničko procesno inženjerstvo, Hinus, Zagreb 2003., M. Hraste,
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