1. komponenta

Lecture type	Total
Lectures	30
Laboratory exercises	30

* Load is given in academic hour (1 academic hour = 45 minutes)

COURSE OBJECTIVE:
The objective of this course is to become familiar with the theoretical principles, practical work and use of instrumental techniques and procedures related to process analysis. The choice of method depends on knowledge of the basic principles of each method or group of methods and an understanding of their advantages and limitations.

COURSE IMPLEMENTATION PROGRAM:
Lectures and seminars:
1. INTRODUCTION: Fundamentals of Process Analysis. Basic principles of instrumental analysis. Signals in process analysis. Validation. Calibration methods (standard addition method, external standard method, internal standard method).
2. INSTRUMENTAL ANALYTIC METHODS: Introduction to instrumental methods of analysis. Classification of methods. Basic concepts and principles.
3. Introduction to spectrometric methods. Classification of spectrometry. Atomic spectrometry (emission (AES), absorption (AAS), fluorescence spectrometry (AFS)).
4. Molecular spectrometry (IR spectrometry, spectrophosphorimetry, spectrofluorimetry, scattering spectrometry, nuclear magnetic resonance (NMR), mass spectrometry).
5. I. part examination
6. Electroanalytical methods. Fundamentals. Department. Potentiometry, electrogravimetry, coulometry.
7. Electroanalytical methods. Polarography, voltammetry, stripping analysis, amperometry.
8. Conductometry. Instrumental separation techniques. Electrophoresis: electroanalytical separation method.
9. II. partial examination
10. Instrumental separation techniques. Chromatography. Fundamentals. Separation. Chromatographic resolution models.
11. Chromatography. Moving and stationary phase. Liquid chromatography. Gas chromatography.
12. Thermal analysis methods (thermogravimetric analysis, differential thermal analysis).
13. PROCESS ANALYSIS: Process analysis, steps in process monitoring, real time measurement. Sampling. Automation of analytical procedures. Flow analysis, analysis by introducing samples into the flow. Automated analytical systems. Related techniques. Process analyzers.
14. III. partial examination
15. Presentation of student seminar papers.

1. Correctly interpret the acquired theoretical knowledge of the methods of instrumental analysis and the principles of operation of instruments, as well as procedural knowledge and skills related to the practical performance of measurements.
2. Explain the relationship between basic knowledge and application in instrumental analysis and process analysis.
3. Compare, interpret and explain the results obtained by the analytical procedure.
4. Integrate acquired knowledge and apply it to problem solving and decision making in analytical practice and process analysis.
5. Evaluate, compare, select, recommend, and conclude which method of analysis is most appropriate for a given real-world problem.

1. LITERATURA POTREBNA ZA POLAGANJE ISPITA:
   1. D. A. Skoog, D. M. West, F. J. Holler, Osnove analitičke kemije, Školska knjiga Zagreb, 1999.
   2. M. Kaštelan Macan, Kemijska analiza u sustavu kvalitete, Školska knjiga Zagreb 2003.
   3. I. Piljac, Elektroanalitičke metode, RMC, Zagreb 1995.
   4. skupina autora, Analitika okoliša (ur. M. Kaštelan Macan, M. Petrović), HINUS i FKIT, Zagreb 2013.
   5. Radni materijal s predavanja.
   6. Radni materijal za vježbe (interna skripta).,
2. DOPUNSKA LITERATURA:
   1. D. A. Skoog, F. J. Holler, T. A. Nieman, Principles of Instrumental Analysis, Saunders College Publishing 1997.,

Enrollment :
Passed : General and inorganic chemistry
Attended : Analytical chemistry
Attended : Physics II

Mandatory course - Regular studij - Chemical Engineering