PURPOSE:
Introducing students to the establishment, development and implementation of quality systems and quality monitoring processes, products and services. The above skills are a prerequisite for participation in the European integration process of exchanging goods, services and information.
THE CONTENTS OF THE COURSE:
Lectures and seminars:
1. Introduction. The quality system. Planning, implementing and documenting quality assurance programs.
2. The elements of the quality system. Quality assurance of the production process. Ensuring the quality of the measuring process.
3. The importance of appropriate measurement process to ensure the quality of processes and products.
(Seminar: computational tasks.)
4. Planning and standardization of the measurement system.
5. Planning and optimization experiments.
6. Sources of errors and their removal.
(Seminar: computational tasks.)
7. The impact of measurement uncertainty on the result of the decision.
(Seminar: computational tasks.)
8. The first partial test.
9. Quality Control. Validation.
(Seminar: computational tasks.)
10. Internal and external quality assessments. Collaborative studies. Reference materials.
11. An independent assessment of the quality system. Certification and accreditation.
12. Improving Quality: diagrams by Ishikawa, Pareto diagram, the method of process analysis.
13. Project management - goals, phases, processes, planning, quality, time and cost. Cost-benefit analysis. Standards and standardization.
14. The second partial test.
15. Seminars students on a given topic.
Laboratory exercises:
(block courses in six periods by 5 hours)
1. Determining the composition of copper alloys classical analysis - determining outliers Q-test.
2. The validation of thin layer chromatography method for determination of pesticides in soil.
3. Comparison of extraction methods for the determination of polyphenols in chocolate - determining the impact of interference from the sample to the chromatographic determination after different methods of extraction.
4. Determination of antibiotics in water by SPE-HPLC-DAD method - the qualitative and quantitative determination of an analyte, and determining the effectiveness of the solid phase extraction.
GENERAL AND SPECIFIC COMPETENCE:
Students gain basic knowledge for establishing quality in the analytical laboratory, as the quality of work in the analytical laboratory to ensure, control and evaluate and apply them to real samples from the environment, in food analysis or other samples (alloys, ores) in accordance with good laboratory practices.
KNOWLEDGE TESTING AND EVALUATION:
Written and oral examination. The possibility of release written part of the exam if you collect enough points.
The oral part of the exam with the teacher.
MONITORING OF THE COURSE QUALITY AND SUCCESSFULNESS:
Student questionnaire.
LITERATURE:
1. LECTURES:
1.) M. Kaštelan-Macan, Kemijska analiza u sustavu kvalitete, Školska knjiga Zagreb, 2003.
2.) Analitika okoliša, ur. M. Kaštelan-Macan i M. Petrović, HINUS i Fakultet kemijskog inženjerstva i tehnologije, Zagreb, 2013.
2. SEMINAR:
Z. Šoljić, Računanje u kvantitativnoj kemijskoj analizi, Sveučilište u Zagrebu, Zagreb 1998.
3. LABORATORY EXERCISE:
D. Ašperger, Interna skripta za laboratorijske vježbe iz kolegija Upravljanje kvalitetom, ZAK, FKIT, Zagreb, 2009.
ADDITIONAL LITERATURE:
1.) J. M. Miller, Chromatography-Concepts and Contrasts, Wiley-Interscience, New Jersey, 2005.
2.) D. A. Skoog, D. M. West, F. J. Holler, Osnove analitičke kemije, Školska knjiga Zagreb, 1999.
3.) K. Eckschlager, K. Danzer, Information Theory in Analytical Chemistry, John Wiley&Sons, Inc., New York 1998.
4.) F. M. Garfield, Quality Assurance Principles for Analytical Laboratories, AOAC, 1991.
Expected learning outcomes at the level of the course:
1. Determine the basic settings of the quality assurance system over the quality of the analytical/production process, products and services.
2. Assess how to establish, implement, control and improve the quality of the analytical/production process, products and services.
3. Critically judge when making a decision, create new ideas, apply the acquired knowledge in practice and, based on the results of quality assurance and application of standards, be guided in evaluating and concluding in the processes of implementing the quality system.
4. Review the results get independent work in the laboratory/production process and recommend the results during the presentations to the interdisciplinary team, and determine and valorize good communication with people who are not experts, but with the possibility of working in an international context.
Learning outcomes at the level of the study programme Materials Science and Engineering:
1. Relate expert knowledge in materials science and engineering with awareness of its societal, economic and environmental impacts.
2. Identify problems in area of materials science and engineering.
3. Apply scientific methods to solve problems in area of materials science and engineering.
4. Analyse information from various sources.
5. Interrelate results from various methods with scientific literature in order to interpret them as well as possible.
6. Select suitable methods and equipment in processing, characterization and application of materials, taking into account work safety.
7. Use various means of communication with scientific and professional community as well as the society at large.
8. Explain results of their work to non-experts, experts in other fields and international partners.
9. Organize their time and work plan on their own.
10. Develop work ethics, personal responsibility and aspiration for further learning.
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- Determine the basic settings of the quality assurance system over the quality of the analytical/production process, products and services.
- Assess how to establish, implement, control and improve the quality of the analytical/production process, products and services.
- Critically judge when making a decision, create new ideas, apply the acquired knowledge in practice and, based on the results of quality assurance and application of standards, be guided in evaluating and concluding in the processes of implementing the quality system.
- Review the results get independent work in the laboratory/production process and recommend the results during the presentations to the interdisciplinary team, and determine and valorize good communication with people who are not experts, but with the possibility of working in an international context.
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LITERATURA POTREBNA ZA POLAGANJE ISPITA:
1. PREDAVANJA:
1.) M. Kaštelan-Macan, Kemijska analiza u sustavu kvalitete, Školska knjiga Zagreb, 2003.
2.) Analitika okoliša, ur. M. Kaštelan-Macan i M. Petrović, HINUS i Fakultet kemijskog inženjerstva i tehnologije, Zagreb, 2013.
2. RAČUNSKI SEMINAR:
Z. Šoljić, Računanje u kvantitativnoj kemijskoj analizi, Sveučilište u Zagrebu, Zagreb 1998.
3. LABORATORIJSKE VJEŽBE:
D. Ašperger, Interna skripta za laboratorijske vježbe iz kolegija Upravljanje kvalitetom, ZAK, FKIT, Zagreb, 2009.,
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DOPUNSKA LITERATURA:
1.) J. M. Miller, Chromatography-Concepts and Contrasts, Wiley-Interscience, New Jersey, 2005.
2.) D. A. Skoog, D. M. West, F. J. Holler, Osnove analitičke kemije, Školska knjiga Zagreb, 1999.
3.) K. Eckschlager, K. Danzer, Information Theory in Analytical Chemistry, John Wiley&Sons, Inc., New York 1998
4.) F. M. Garfield, Quality Assurance Principles for Analytical Laboratories, AOAC, 1991,
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