PURPOSE: The aim of this course is to introduce the theoretical principles, practical work and use the instruments of equipment and procedures for instrumental methods of chemical analysis. The choice of method will be depend on knowledge of the basic principles of individual method or group of methods and the understanding of their benefits and limitations.
THE CONTENTS OF THE COURSE:
Lectures:
1. Introduction into the program of course, instructions for work in the laboratory. Introduction - types of analytical signals, the basic components of instruments, instrumentation development, and classification of instrumental methods.
2. Spectrometry, history of spectroscopic techniques, fundamentals of spectrometry, a classification of spectrometry - molecular and atomic spectrometry.
3. Classification of spectrometry considering the result of interaction of the sample with energy: absorption, induced absorption, emission, polarization of EMR, scattering, mass to charge ratio.
4. Spectrometry radiation of electrons and ions, and mass spectrometry.
5 The first partial test.
6. Electroanalytical methods - history, fundamentals, classification, electrochemical cell.
7. Potentiometry, conductometry, electrogravimetry.
8. Voltammetry, amperometry, coulometry.
9. Electrophoresis - fundamentals, classification, capillary electrophoresis.
10. The second partial test.
11. Separation instrumental methods, chromatography - introduction, basics, classification of chromatography, gas chromatography.
12. Liquid chromatography, chromatography at the super critical conditions, planar chromatography, ion chromatography, size exclusion chromatography.
13. Thermal methods.
14. The third partial test.
15. Presentation of seminar papers.
Laboratory:
1. UV/VIS spectrometry - determination of iron and/or chromium - the method of external standards.
2. EMR scattering spectrometry - turbidimetric determination of sulfate.
3. Atomic absorption spectrometry - determination of copper content - method of standard addition.
4. Potentiometry: potentiometric titration and data processing - determination of salicylic acid.
5. Direct potentiometry - determining the concentration of chloride or fluoride.
6. Conductometry - determination of acids mixture by conductometric titration.
7. Compensation of laboratory exercise.
GENERAL AND SPECIFIC COMPETENCE:
Introduction to instrumental methods, and connect with process analysis.
KNOWLEDGE TESTING AND EVALUATION:
Written and oral examination. The possibility of release written part of the exam if you collect enough points.
The oral part of the exam with the teacher.
MONITORING OF THE COURSE QUALITY AND SUCCESSFULNESS:
Student questionnaire.
LITERATURE:
1. D. A. Skoog, D. M. West, F. J. Holler, Osnove analitičke kemije, Školska knjiga Zagreb, 1999.
2. M. Kaštelan-Macan, Kemijska analiza u sustavu kvalitete, Školska knjiga Zagreb 2003.
3. I. Piljac, Elektroanalitičke metode, RMC, Zagreb 1995.
4. Radni materijal s predavanja.
5. Radni materijal za vježbe (interna skripta).
ADDITIONAL LITERATURE:
1. Analitika okoliša, ed. M. Kaštelan-Macan i M. Petrović, HINUS and Fakultet kemijskog inženjerstva i tehnologije, Zagreb, 2013.
2. J. M. Miller, Chromatography-Concepts and Contrasts, Wiley-Interscience, New Jersey, 2005.
3. K. H. Koch, Process Analytical Chemistry. Control, Optimization, Quality, Economy, Springer Verlag, Berlin 1999.
4. D. A. Skoog, F. J. Holler, T. A. Nieman, Principles of Instrumental Analysis, Saunders College Publishing 1997.
Expected learning outcomes at the level of the course:
1. To connect, evaluate and distinguish the adopted theoretical knowledge related to the methods of instrumental analysis and the principles of operation of instruments.
2. Generate and integrate procedural knowledge and skills related to the practical performance of measurements.
3. Design and set a hypothesis of the connection of basic knowledge with the application in instrumental analysis.
4. Plan and organize independent work on instruments in the laboratory for instrumental analysis, and further learn independently having a positive attitude about the need to develop professional competencies.
5. Present the acquired knowledge and develop and compile a proposal in problem solving and decision making in analytical practice.
Learning outcomes at the level of the study programme Applied Chemistry:
1. Evaluate chemical information and data.
2. Present material related to the study programme in writing and orally, to an informed audience.
3. Analyse chemical information and data using a computer.
4. Apply knowledge in practice, in particular in problem-solving, relating to both qualitative and quantitative information.
5. Retrieve information through on-line computer searches.
6. Apply standard laboratory procedures and instrumentation in synthetic and analytical work, in relation to both organic and inorganic systems.
7. Apply techniques and methods to measure chemical properties, events or changes.
8. Interpret data derived from laboratory observations and measurements in terms of their significance and relation to appropriate theory.
9. Demonstrate capability to engage in interdisciplinary teamwork.
10. Plan time managing.
11. Organise autonomous work.
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LITERATURA POTREBNA ZA POLAGANJE ISPITA:
1. D. A. Skoog, D. M. West, F. J. Holler, Osnove analitičke kemije, Školska knjiga Zagreb, 1999.
2. M. Kaštelan-Macan, Kemijska analiza u sustavu kvalitete, Školska knjiga Zagreb 2003.
3. I. Piljac, Elektroanalitičke metode, RMC, Zagreb 1995.
4. Radni materijal s predavanja.
5. Radni materijal za vježbe (interna skripta).,
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DOPUNSKA LITERATURA:
1. Analitika okoliša, ur. M. Kaštelan-Macan i M. Petrović, HINUS i Fakultet kemijskog inženjerstva i tehnologije, Zagreb, 2013.
2. J. M. Miller, Chromatography-Concepts and Contrasts, Wiley-Interscience, New Jersey, 2005.
3. K. H. Koch, Process Analytical Chemistry. Control, Optimization, Quality, Economy, Springer Verlag, Berlin 1999.
4. D. A. Skoog, F. J. Holler, T. A. Nieman, Principles of Instrumental Analysis, Saunders College Publishing 1997.,
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